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Sensitivity increases with decreasing liquid solid ratios and contact time during percolation.
Batch experiments were conducted at T = 150°C (± 1°C) and solution:solid ratios of 10 1 and 5 1.
Different liquid:solid ratios, alkali concentrations and Na2O:ash ratios were tested.
The experimental data were obtained for various liquid binder (water) to solid ratios, screw speeds, material throughputs, and screw configurations.
XRD data for the batch reactions at solution:solid ratios of 10 1 and 5 1 are shown in Figures 10 and 11 and plots of the extent of reaction are shown in Figures 12 and 13 (T = 150°C).
This is quite different from situations with low solution volume to solid ratios where similar calculations show that it is difficult to remove adsorbed ions by solution replacement [41].
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Water to solid ratio was 7.69 1.
Figure 6 29 Si MAS NMR of batch reactions at a solution:solid ratio of 10 1.
Optimized extraction conditions were extractant/ solid ratio 12: 1 (v w), 150 rpm agitation speed and 40°C.
The liquid to solid ratio (LS) reached in the experiment was 0.63:1.
Three independent variables, extraction temperature, extraction time and water to solid ratio were investigated.
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