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It is clear from Table 1 that the particle size obtained from FETEM measurements corroborates well with the crystallite size obtained from XRD analysis.
The mean TiN crystallite size obtained was 10 nm for the AlN TiN composition.
The average particle size, obtained by transmission electron microscopy, ranged between 4 and 20 nm.
The mean particle size obtained by ball milling was over the nanometric range (day 1).
Figure 2 Histogram and distribution of segment size obtained from Figure1.
This value is consistent with nanofiber size obtained by TEM analysis as shown in Figure 3.
For comparison, size obtained from the HRTEM analysis is also shown in Figure 1g.
The crack size obtained is denoted as (a_{i} left( {t_{0},xi } right)).
This is in fair agreement with the particle size obtained from X-ray diffraction measurements.
These results agreed with the particle size obtained from the TEM images.
delta, =, 1/D^{2} (2 where D is the crystallite size obtained from W H plot.
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