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The effects of sintering schedule on crystalline phase assemblage and thermomechanical properties were investigated.
When the chemistry and sintering schedule is carefully controlled, the intergranular phase is a crystalline RE2Si2O7 phase, which imparts improved mechanical and oxidation properties to the Si3N4.
The effect of particle size distribution, binder content, processing parameters, and sintering schedule on the microstructure and mechanical properties of porous constructs was investigated.
It was demonstrated that by changing the composition and sintering schedule, the theoretical density of CaZr4(PO4)6 could be reached through liquid phase sintering and the thermal expansion characteristics can be engineered as desired by controlling its composition and sintering schedule.
It was determined that 1 wt.% addition of Li2CO3 with accelerated sintering schedule produced the theoretical density of CaZr4(PO4)6 and further addition of Li2CO3 rapidly decreased the sintered density.
The dielectric properties characterized from room to high temperature (RT– HT, up to 600 °C) revealed: (i) noticeable effects of sintering schedule on dielectric constant (5 10) and dielectric loss factor (~0.02 0.04); (ii) stable dielectric properties until the failure of the electrode material.
Similar(54)
The suitable forming parameters and sintering schedules were identified from this study.
The defect free green compacts were sintered in inert gas fired sintering furnace for different sintering schedules.
This paper presents the effects of forming parameters and sintering schedules to the mechanical properties and microstructures of products formed through warm compaction route.
The influence of sintering temperature and heating schedule has been investigated.
It has limitations such as long heating schedule at high sintering temperature of about 1300 °C, higher obtained grain/particle size, and higher time consumption.
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