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Using MiríadaX statistics, Table 3 shows completion rates for total enrolment, the number of participants who entered the course at least once and the number who started at least the first training module.
Table 1 shows completion rates of Type 2 diabetes audits by year of commencement in the project.
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The reaction mixture was stirred at room temperature for 5 8 h until TLC analysis showed completion of the reaction.
The crude 19 was dissolved in 2 N HCl (15 mL), and the mixture was stirred until TLC analysis showed completion of the reaction.
Anhydrous K2CO3 (3.5 equiv) and substituted benzyl bromide (1.5 equiv) were added to a solution of compound 12 in acetonitrile (30 mL), and the reaction solution was then stirred at room temperature until TLC analysis showed completion of the reaction.
The reaction mixture was refluxed for 2 h, then anhydrous K2CO3 (3.5 equiv) and Boc2O (1.5 equiv) were added to the reaction solution, and the mixture solution was stirred at room temperature until TLC analysis showed completion of the reaction.
To a solution of 7a (5 mmol) in anhydrous CH2Cl2 (20 mL), TsCl (5 mmol), TEA (10 mmol) and dimethylamino pyridine (0.5 mmol) were added and stirred at room temperature until the TLC showed completion of the reaction.
The crude 17 (1.0 equiv), TBSCl (1.2 equiv) and imidazole (1.5 equiv) were used to synthesize compound 18 in CH2Cl2, after reaction was complete, 3-nitrobenzyl bromide (3.0 equiv) and TEA (3.0 equiv) were added to the reaction solution, which was stirred at room temperature until TLC analysis showed completion of the reaction.
The mixture was stirred at room temperature until TLC showed completion of reaction.
The reaction was monitored by IR spectroscopy (νCO) showing completion after approximately 20 h.
Different incubation times were also investigated, showing completion of the reaction after 1 h at room temperature.
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