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The produced radioactivity is recovered from the target wall via a double shoot method.
Quantitative analysis of aflatoxin content in culture filtrates was performed by a "dilute and shoot" method as described by Kovač et al. (2017).
A total of 90 projections (step and shoot method, 35 s per projection, 64 × 64 matrix, total imaging time 23 min) were obtained over a 360° circular orbit.
A 20% window was used around the 140-keV energy peak of 99mTc-tetrofosmin and 90 projections (step and shoot method, 35 s/projection, 64×64 matrix, total imaging time 23 min) were obtained over a 360° circular orbit.
Various SPE cartridges (Oasis HLB and MAX, Sigma Supel-Select HLB, Sequant ZIC-HILIC, Bakerbond Polar Plus) have also been tested during method development of the established dilute and shoot method but failed to retain the polar glucuronide conjugates, with the exception of the Oasis HLB [ 16] and the ZIC-HILIC cartridges when using optimized protocols.
Reference standards, which have been chemically synthesized and confirmed by NMR, were used to establish a liquid chromatography-electrospray ionization (LC-ESI -MS/MS-based "diLC-ESI -MS/MS-basedhod for the detection, unambiguous identification, and quantification of both suLC-ESI -MS/MS-based wheat extracts.
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Chamberlain adopted the underhand shooting method popularized by Rick Barry, one of the deadliest free-throw shooters in N.B.A. history.
This study demonstrates that optimized radionuclide production, via a proton double-shoot method on [18O]2 leads to significant higher amounts of FDOPA with higher specific activity.
The installation of a Cyclone 18 twin cyclotron (IBA, Belgium) recently allowed us to change our [18F]F2 production method from the 20Ne d,α)18F single-shoot method (De Vries et al. 1999) to the 18O p,n)18F double-shoot method (Bishop et al. 1996).
Intensive cleaning of the target using flushing and vacuum was always done after the first shoot and therefore the [18F]F2 produced via the double-shoot method may contain less chemical impurities and therefore its reaction with the [18F]FDOPA precursor appears to be more efficient.
As the Cyclone 18 twin cyclotron has a newly designed small volume target, the double-shoot production method needs less carrier F2 gas, which increases the specific activity of [18F]F2 in comparison to the single-shoot method using an MC17 Scanditronix cyclotron.
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