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TMS contained in CDCl3 served as shift reference.
Chemical shifts were given in ppm with acetone as the internal chemical shift reference.
Thus, 'Madagascar' was able to shift reference from the mainland to the island once perceptually-based groundings in the island became established.
New methods for using inorganic phosphate buffer as an internal pH reference, involving mathematical correction factors and careful control of the chemical shift reference sample, are illustrated.
The TSP (trimethyl-silil-propionate) was used as an external chemical shift reference.
Metabolites were quantified by comparison to the internal standard DSS, which also served as a chemical shift reference.
Similar(20)
Samples contained 0.05%% (v/v) TMS for chemical shift referencing.
Spectral chemical shift referencing on the TSP signal at 0 ppm was performed for all spectra.
4,4-dimethyl-4-silapentane-1-sulfonic 4,4-dimethyl-4-silapentane-1-sulfonic 4,4-dimethyl-4-silapentane-1-sulfonic 4,4-dimethyl-4-silapentane-1-sulfonic 4,4-dimethyl-4-silapentane-1-sulfonic 4,4-dimethyl-4-silapentane-1-sulfonic
Samples contained 0.5 mM DSS-d6 for chemical shift referencing and as an internal standard for quantification.
All NMR samples contained 5% H2O for deuterium locking and 0.5 mM DSS (4,4-dimethyl-4-silapentane-1-sulfonic 4,4-dimethyl-4-silapentane-1-sulfonic 4,4-dimethyl-4-silapentane-1-sulfonic 4,4-dimethyl-4-silapentane-1-sulfonic 4,4-dimethyl-4-silapentane-1-sulfonic 4,4-dimethyl-4-silapentane-1-sulfonic
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