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The experimental design consists of four parameters (pouring temperature, shearing temperature, shearing time and shearing rate) with three levels.
The contribution of each parameter shows that pouring temperature is the most significant parameter affecting the grain size, and the shape factor highly depends on the shearing temperature.
The concentration of precursors is observed to reduce with increasing shearing temperature, as evidenced by twisting degree of lamellar crystals after isothermally crystallized at 127 °C.
The optimized rheo-casting processing parameters are 650 °C for pouring temperature, 585 °C for shearing temperature, 40 s for shearing time, and 600 r/min for shearing rate.
In this work, the solidification behaviour of AZ91D alloy under intensive forced convection in the RDC process was investigated experimentally to understand the effects of the intensity of forced convection, shearing time and shearing temperature on the nucleation and growth behaviour.
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The effects of shear temperature and shear rate were systematically studied.
As expected, β-phase crystallinity, long period and lamellar thickness are steadily dependent on the shear temperature and shear rate.
The data obtained revealed also close correlations between annealing time, shear temperature and incubation time.
The final crystallinity of SC increased to as high as ∼45% with a shear rate of 178 s−1 when the shear temperature was 150 °C.
Multiple factors influence the crystallization of SC and α crystals, including the shear rate, shear temperature and the nucleating/confinement effect of SC on α crystals.
At lower shear temperature (i.e., 160 °C), β-phase crystallinity, long period and lamellar thickness were further decreased with increasing the shear rate.
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