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These polymer-based materials also suffer from exothermic setting reactions (Vallo et al. 1999).
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Setting reaction has been followed with time resolved infrared spectroscopy, supported by 2D correlation spectroscopy.
Wood treatments are multivariable processes required for the appropriate cement setting reaction on wood surfaces.
The setting reaction of the cement was followed using magic angle spinning nuclear magnetic resonance (MAS-NMR) spectroscopy.
Such an explanation can be related to the setting reaction of zinc phosphate cements.
A likely explanation is that as time passed the setting reaction became more complete.
The setting reaction of FT was accellerated with a 40s photo-activation.
The microhardness measurements are an indicator of the maturity of the setting reaction [ 19, 24].
The methacrylate groups enable a rapid crosslinking setting reaction but lactide segments ensure subsequent degradability.
A possible explanation is that some of the ions, for example phosphate ions, diffused into the cement and pushed the setting reaction toward an increased precipitation reaction.
The results are shown in Figure 5 where blue, red and green dots represent training set, test set and prediction set reactions, respectively.
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