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Before structural refinements, 5% randomly selected reflections were set aside for calculating Rfree as a monitor [ 11].
Set aside for 20 minutes.
The part set aside for Rose presumably?
Set aside for 1/2 hour.
Set aside for 15 minutes.
Set aside for a moment.
Set aside for 10 minutes.
Set aside for 10-15 minutes.
Set aside for 30 minutes.
Set aside for about 15 minutes.
Refinement was performed with the native data to a resolution of 2.75 Å using the program PHENIX [54] with a random 1.5% of all data set aside for an Rfree calculation.
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