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This phase segregation decreased when hard segment content increased.
The hard segment content was varied minimally and the B3 monomer was also varied.
As expected, increasing the hard segment content increased the stiffness and the flow stress levels.
Changes in macromolecule order with increasing hard segment content were observed via modulated differential scanning calorimetry.
These techniques collectively show that the urea aggregation increases as the hard segment content is increased.
The amount of water to achieve liquid demixing increased systematically with the hard segment content.
Silicone urea copolymers with urea hard segment content between 10 and 42% by weight were prepared.
The morphology of a TPU with a high hard segment content was investigated.
All copolymers had a constant urea hard segment content of 15% by weight.
Scanning electron micrographs of the xerogel revealed a 3D-network structure – higher hard segment content P1000-1 3.55) led to a fibrous morphology and lower hard segment content P2000-1 33) led to a microsphere like architecture.
The biocompatibility results indicated that proliferation of human bone-derived cells (HBDC) cultured in vitro improved with increasing hard segment content while the osteogenic potential of HBDC decreased with increasing hard segment content.
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