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In a sequence of modification steps one of the electrodes was covered first with a positively charged Ni porphyrin entrapped into a negatively charged electrodeposition paint followed by the manual modification of the second working electrode by a bienzyme sensor architecture based on crosslinked redox hydrogels with entrapped peroxidase and glutamate oxidase.
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A new electrode, comprising a dual working electrode (W1 and W2) in which the area of W1 was one-tenth the total working electrode area, was developed.
The working electrode was first immersed in the test solution for 60 min to establish a steady state open circuit potential.
The working electrode was first immersed into the test solution for 60 min to establish a steady state open circuit potential.
Before immobilization of MP-11, the Au working electrode was first modified by a self-assembled monolayer of 1-undecanethiol (UDT).
The CNT working electrode was first electrochemically oxidised to yield a hydroxyl terminated surface, which was subsequently silanized to produce an amine terminated CNT.
Layer i: The working electrode was first coated with poly m-phenylenediamine (m-PD) using electropolymerization, to screen out potential interferences.
A drop (4 μL) of the Tris hCl solution of ZBW1 (5 × 10−3 M) was first dripped onto the graphene functionalized working electrode area of SPE, dried under vacuum, and then the Nyquist plots were recorded.
Branched zinc oxide nanorods (BZR) arrays, an array with high charge carries collection efficiency and specific surface area, are grown on the reduced graphene oxide-paper working electrode for the first time to construct a paper-based electrochemical (EC) immunosensor.
The second two-electrode design utilizes an ultramicrodisk working electrode which faces a large surface area silver-disk semireference/counter electrode.
The working electrode was prepared by first printing carbon ink onto a sheet of polyimide using the flexographic printing technique.
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