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Another IOL was opacified in the original sealed vial.
For CO2 and H2 analyses, 0.5 mL of fluid sample was directly introduced to each Ar-purged, sealed vial at room temperature.
For the analysis of H2 concentration, approximately 0.5 ml of fluid was directly introduced into an Ar-purged, sealed vial without air contamination at room temperature.
The sealed vial was then fully immersed in a temperature-controlled water bath, model Grant GD200, (Grant Instruments, Cambridge, UK), and allowed to thermostatize.
The sealed vial was baked at 530°C for 6 hours, and the graphite produced (∼1 mg) was pressed and loaded into the ion source of the accelerator.
Switching experiment: CDCl3 (0.5 mL) was added to a sealed vial containing rotaxane [ 4AuCl] (7.1 mg, 0.0062 mmol) and AgSbF6 (2.2 mg, 0.0062 mmol).
Similar(13)
A 15 μL aliquot of each solution was trimethylsilylated at room temperature using 50 μL of N,O-bis trimethylsilyl -trifluoroacetamide (BSTFA, Sigma-Aldrich) iN,O-bis trimethylsilyl -trifluoroacetamideg to the supplier's recommeN,O-bis trimethylsilyl -trifluoroacetamide
3 ml of 0.2 micron filtered exhaled breath sample was transferred into a 10ml septa-sealed vial containing helium gas, and analyzed by gas isotope ratio mass spectrometry using a DeltaplusXL instrument for 13C enrichment in headspace CO2.
Zn mirror-2 appeared to have a crystal structure and stuck to the septa-sealed vial.
Furthermore, the remaining Zn dust appeared as a Zn cake stuck to the bottom of the septa-sealed vial.
(13) The flame-sealed quartz tube was replaced with a septa-sealed vial, which increased the throughput to 150 samples per d/skilled analyst.
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