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The ampoules were then sealed under vacuum at a pressure of less than 0.1 mTorr.
The ampoule was sealed under vacuum and heated up to 900 °C in a rocking furnace for 10 h followed by quenching into water from 700 °C.
Samples of amorphous Zr55Cu20Al10Ni10Pd5 alloy with rectangular section and 2 mm thickness, sealed under vacuum in specially designed quartz tubes were studied.
Then, the ampoules were degassed, sealed under vacuum condition, and maintained at 70°C ± 1°C in a water bath and shaken using a shaker for about 24 h.
The apparatus can be sealed under vacuum in its upper part.
The NMR tube was sealed under vacuum and placed into a plastic straw for measurements.
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The ampoules were again evacuated, flash frozen in liquid nitrogen, and immediately heat-sealed under vacuum using a glassblower's torch.
The ampoule was sealed under a vacuum and heated at 900 °C in a rocking furnace for 10 h, followed by quenching into room temperature water from 700 °C.
Then, the ampoules were sealed under a vacuum, heated up to 900 °C with 2 °C/min rate and stayed at this temperature for 10 h in a rocking furnace with further quenching into water from 700 °C.
For the 75:25 albumin-glycerol bioplastics, the spotted surface of the broken plastic was the aspect of highest interest as these images could have been the evidence of glycerol leaching from the plastic on a much smaller scale, with the moisture being removed from the sample when the SEM chamber was sealed under high vacuum (Figure 8b).
The chamber was sealed under partial vacuum (>600 Torr) and placed within the beam path of the DRIFTS cell.
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