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For each sample, 82 scans in the range 1000 2500 nm at a 1.32 nm nominal resolution were acquired.
Each spectrum was obtained by co-adding 64 scans in the range from 4000 to 525 cm−1, at a resolution of 8 cm−1.
Each spectrum resulted by the co-addition of 64 scans in the range 4000 525 cm−1 at a resolution of 8 cm−1.
Wavelength scans in the range of 200 250 nm were performed in rectangular quartz cells (JASCO model: T-11-ES-1) with a path length of 0.1 cm.
The SiO2 and SiO2 POOH were analyzed by Fourier transform mid-infrared (FTIR) spectroscopy (Prestige-21; Shimadzu, Japan) at a resolution of 4 cm−1 and 24 scans in the range of 700 2500 cm−1.
FTIR spectrometer via the attenuated total reflection (ATR) at a resolution of 4 cm−1 and 32 scans in the range of 400 4000 cm−1 at room temperature.
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The material was scanned in the range of 10o 80o.
The samples were scanned in the range 20° 80° of 2θ with a scanning speed of 2°min−1.
The samples were scanned in the range from 10to9090 degrees 2-theta.
The sample was scanned in the range of 10° to 80° at a scan rate of 2°/min.
The investigations were carried out by automatic step scanning in the range of scattering angles (2θ) from 2.6° to 40°, and the exposure time was 5 s.
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