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The investigations were carried out by automatic step scanning in the range of scattering angles (2θ) from 2.6° to 40°, and the exposure time was 5 s.
Mass spectra were obtained in EI mode (70 eV), scanning in the range 45 650 m/z, with a cycle time of 0.2 s.
Mass spectra were obtained in EI mode (70 eV) scanning in the range of m/z 45 to 850 with a cycle time of 1 s.
As shown in Figure 6, slow step scanning in the range of approximately 92.5° to 97.5° of 2θ was conducted for ψ-angles in the range of 0° to 45°.
The bacterial cells suspended in Phosphate buffered saline (PBS pH 7.2) and cell-free supernatant were subjected to spectrum scanning in the range of 300 700 nm using a UV VIS spectrophotometer (Shimadzu UV 1800) and acidified methanol was used as a blank.
The structural characterization of the as-synthesized and heat-treated powders was carried out by Philips X-ray diffractometer (model 3710; Koninklijke Philips N.V., The Netherlands) using Cu Kα radiation (λ = 1.5405 Å) at room temperature by continuous scanning in the range of 2 to 85 θ° to analyze the phase and crystallite size.
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The material was scanned in the range of 10o 80o.
The samples were scanned in the range 20° 80° of 2θ with a scanning speed of 2°min−1.
The samples were scanned in the range from 10to9090 degrees 2-theta.
The sample was scanned in the range of 10° to 80° at a scan rate of 2°/min.
Each spectrum resulted by the co-addition of 64 scans in the range 4000 525 cm−1 at a resolution of 8 cm−1.
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