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This paper describes the fabrication of porous silicon nitride ceramic materials using a fugitive additive, corn starch, which allows samples to be produced with different volume fractions of porosity from ∼0 to 0.25.
The technical requirements of IS-ARTS (mass, power and number of samples produced) depend strongly on the sample mechanical properties, sample processing rate, the sample size and number of samples to be produced.
This study shows that for the studied materials, the samples cored in the plate are the most homogeneous, the ones produced by gyratory compaction yield scattered results but rather homogeneous samples can be obtained by respecting geometry criteria for the samples to be produced, and by sawing the edges where the compaction is the least efficient.
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The technology suggested allows a composite sample to be produced with the permeability of 2.8, and low magnetic loss at frequencies below 1 GHz, the volume fraction of Fe is as low as 0.77%.
As the 1st additional step to HCD process in MBD/UM, a product sample has to be produced on the basis of the design solution.
The Wilhelmy plate methodology was particularly suitable for both quantifying liquid zinc wetting and producing coated samples to be characterized.
With regard to each sample size, 1,000 Monte Carlo samples are produced to reveal the stochasticity of the estimated parameters.
Moreover, 12 × 12 × 2 cm mortar samples were produced to apply radiation shielding test.
Additional carbon-doped Ni samples were produced to understand the influence of carbon on the saturation microstructure.
Both types of samples were produced according to an experimental design.
The samples were produced according to two methods: for different pressures with constant temperature and at different temperatures with constant pressure.
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CEO of Professional Science Editing for Scientists @ prosciediting.com