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A pycnometer suited to the samples dimensions was constructed and calibrated.
To quantify the mechanical effects of variability on the characteristic strength and the effects of the samples dimensions, the random and spatial variation are firstly explored interpreting field and laboratory tests with the Random Field theory.
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Sample dimensions were unaffected by annealing.
Gage length and sample dimensions were measured and samples were approximated as a rectangular cross-section.
Sample dimensions, namely column diameter, stated here differ slightly from those published in11,12 due to more precise and accurate SEM measurement performed with a conductive polymer.
For real sample sizes, proper material characterization requires determining the effect of finite sample dimensions.
Changes in sample dimensions alone produced widely different values for compressive plasticity.
Conversely, strain hardening is suppressed when confining sample dimensions dominate plastic flow for D/Leff<1.5.
Influences of model parameters and sample dimensions on the predictions are also discussed.
The method is based on measurements of porosity, accurate measurements of the sample dimensions.
This edge effect becomes critical if the sample dimensions are comparable to the thickness of the sample window.
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