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The auto sampler was cooled at 10 °C.
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After pretreatment, the sample was cooled down to 100 °C and saturated with NH3.
The sample was cooled at 80 K.
(3) Each sample was cooled separately to room temperature.
During measurement, the sample was cooled using a cryojet.
The final solid sample was cooled to room temperature.
After 1 h, the sample was cooled to room temperature and the black sample was collected.
After the sample was cooled at the room temperature, 0.268 mL furfuryl alcohol was added.
After the pretreatment, the sample was cooled to 100 °C and saturated with NH3 gas.
The sample was cooled to liquid nitrogen temperature using a cryostat cell (Linkam, THMS 6000).
In all the measurements, the sample was cooled in an optical cryostat to 7.5 K.
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