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Other required data such as weight of saturated and dry core sample were put in the software.
Five microliters of the sample were put on a carbon film supported by a copper grid and blotted with filter papers to obtain a thin liquid film on the grid.
Dried and pulverized samples were carbonized using muffle furnace, a carefully weighed 25.0 ± 0.01 g of raw sample were put into a beaker containing 500 cm3 of 0.3 M ortho-phosphoric acid (H3PO4).
For the determination of Al, Ti and Fe quantities, 10 mL aliquots stock solutions of each sample were put into a 250 mL conical flask to which were added 25 mL of 0.01M EDTA for the formation of Al-EDTA, TiO-EDTA and Fe-EDTA complexes.
Two drops of pellet from each sample were put onto a slide for homogenous smear preparation.
Ten milligrams of the sample were put into platinum crucibles with lids on a high accuracy DSC-cp sample holder of a thermal analyzer (TG/DSC STA449, NETZSCH Instruments Co. Ltd., Germany), after which they were heated from ambient temperature to 800°C at rates of 10, 30 and 50°C/min in the furnace under a nitrogen atmosphere of 80 ml/min.
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When an athlete is tested for drugs, the urine sample is put in two containers.
The sample was put into the UHV TOF-PAES spectrometer in the as-received condition.
Finally, the sample was put under 5% H2/Ag and again scanned.
The sample is put face down on a coplanar waveguide (copper, width of central conductor 600 μm).
Then, the AAO sample was put on a glass slide.
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