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The sample was cooled at 80 K.
(3) Each sample was cooled separately to room temperature.
During measurement, the sample was cooled using a cryojet.
The final solid sample was cooled to room temperature.
And then, the sample was cooled and boiled with hydrochloric acid for 20 min.
After the annealing process, the sample was cooled down to room-temperature.
After the pretreatment, the sample was cooled to 100 °C and saturated with NH3 gas.
After the sample was cooled at the room temperature, 0.268 mL furfuryl alcohol was added.
After 1 h, the sample was cooled to room temperature and the black sample was collected.
The sample was cooled to liquid nitrogen temperature using a cryostat cell (Linkam, THMS 6000).
In all the measurements, the sample was cooled in an optical cryostat to 7.5 K.
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