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In the region near the ultimate tensile strength, these micro defects in the middle of the sample start to grow and build up pores as for example shown in Fig. 12.

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The sample starts to conduct at P ≈ 50 GPa.

The LiBH4/AC sample starts to release hydrogen from just 220 °C, which is 150 °C lower than the onset dehydrogenation temperature of bulk LiBH4.

The dehydrogenated Mg-Al-Ti-F-doped sample starts to take up hydrogen at room temperature with the 6.3 wt% amount of H2 at 150 °C, which is greatly superior to that of the pristine sample.

The arrow indicates that the sample starts to illuminate at around E = 2 kV/cm.

With more Zr doping such as 5%, the PL intensity of Zr/N-TiO2 sample started to increase again.

As the entire sample starts to loss its strength to support differential/shear stress, it is subjected to macro/bulk yield, and plastic deformation and/or viscous flow begins.

However, no primary preventive (initiation prevention) effect was found as in both groups 5.0% of the prospective sample started to smoke (table 3).

While during the low strain rate test true flow stresses between 2 and 2.3 GPa were achieved, the sample starts to plastically deform in the high strain rate test at ≍3.5 GPa and finally fails at stresses exceeding 4 GPa.

These hyperquenched samples start to relax, exothermically, far below the glass temperature, at a temperature (0.75Tg) where the thermal energy permits escape from the shallow traps in which the system becomes localized during hyperquenching.

For reflection above 600 nm, both 405°C and 438°C samples start to exhibit interference effects.

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