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Meanwhile, the RSD of the peak areas in the sample stability test was less than 2.58%.
Freeze and thaw stability and processed sample stability also fulfilled the acceptance criteria.
This suggests that sample stability against oxidation is increased, as discussed in reference [23].
Recovery of various species and sample stability under the applied conditions were also discussed.
Sample stability for upto 16 h was demonstrated, allowing autoinjection cycles to be performed.
It also improved sample throughput and conferred sample stability as well as repeatability from run to run.
Sample stability was confirmed when a change of less than 15% of the analyte concentration was observed [29].
Sample stability and inter- and intrasubject variability were evaluated in the urine of normal and OA populations.
At last, method validation including determination of injection precision, repeatability, and a sample stability test, was performed.
Variation in the duration of transport to central laboratories needs to be considered by ensuring sample stability and proper storage conditions.
A relatively moderate spin rate ranging between 3 and 6 kHz is thus recommended, in order to reach best compromise between resolution and sample stability.
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