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A high-pressure Hg lamp (HB400X-15 400 W; SEN LIGHTS CORP) in a quartz water-cooling jacket was placed at the centre of a 500-mL reaction vessel containing the sample solution for internal irradiation.
The relative standard deviation (RSD) of the proposed method for the extraction and determination of 5 μg THP from 200 μl standard sample solution for 3 replicate measurements was 3.5%.
The 0.1% DMSO solution was used instead of sample solution for blank experiments (ΔAblank/min).
Fig. 5 Growth trend of out of estimation sample solution for output (2000 = 100).
The precision was determined by injecting the same sample solution for six times in 1 day.
The chromosome in Table 1 represents a sample solution for the problem with three different production lines and 50 different types of products.
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Prof Hearst: Sample Solutions for Q2 and Q4, along with grading guidelines.
The sample solutions for cation analysis were stored in the fridge prior the analysis.
Table 3 represents the electrical conductivity, salinity, and sodium-chloride ion concentration values in 100 ml of feed sample solutions for both RPSu-PVP and PSDVB-based IEM systems, respectively.
Since no additional peaks were found in the chromatogram with no reduction in the peak area, this indicates stability of both standard and sample solutions for about 20 hr.
The sample solutions for the UHPLC analyses, including the EEDS (2,000 μg/mL, 80%% methanol), ethyl acetate (EtOAc) fraction (2,000 μg/mL, 100%% methanol), and helveticoside (100 μg/mL 100%% methanol) were filtered (Millex-FG 0.2 μ m, Millipore) prior to the injections.
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Justyna Jupowicz-Kozak
CEO of Professional Science Editing for Scientists @ prosciediting.com