Exact(60)
a TEM sample prepared by FIB.
The sample prepared using pH = 8 had the highest transmittance.
By analyzing both the samples, sample prepared using PF act as better surfactant than sample prepared using WF.
The sample prepared using ethanol shows the best catalytic performance.
The sample prepared by impregnation method has the lowest reducibility, and the sample prepared by sol-gel method shows the highest reducibility.
For example, at 5 min, the sample prepared with H3PO4 underwent 21.6 % weight loss (Fig. 6a), whereas the sample prepared with Na4P2O7 underwent 15.6%% weight loss (Fig. 6d).
Among the samples prepared with SPS, the sample prepared at 1200 °C exhibits a slightly larger Seebeck coefficient than that of the sample prepared at 900 °C.
Among the SPS samples, the thermal conductivity of the sample prepared at 900 °C is about a half of that of the sample prepared at 1200 °C.
The sample prepared under optimized conditions was compared to that synthesized by PEG surfactant.
This is significantly higher than that of the sample prepared by the traditional hydrothermal method.
The sample prepared with SPS at 1200 °C contains minor impurity, Mg1−x Fe x O.
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