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An FT-IR specimen which could be subjected to multiple freeze-thaw cycles could be prepared by the self-designed test sample preparation device.
Packed with polymeric particle, the resulting particle-packed needle was employed as a miniaturized sample preparation device for the analysis of typical volatile organic compounds in tobacco smoke.
A novel needle-type sample preparation device was developed for the effective preconcentration of volatile organic compounds (VOCs) in indoor air before gas chromatography mass spectrometry (GC MS) analysis.
Introducing a bundle of polymer-coated filaments as the extraction medium, the needle was further applied as a novel sample preparation device containing simultaneous derivatization/extraction process of volatile aldehydes.
Miniaturized needle extraction device has been developed as a versatile sample preparation device designed for the rapid and simple analysis of smoking-related compounds in smokers' hair samples and environmental tobacco smoke.
Sources of potential error include human (sample preparation), device (1000 mL graduated cylinder) and the atomic absorption spectrophotometry assay.
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He adds, "We're good at the chemistries and making sample preparation devices, but what do we do if the scale goes from 20 samples a day to 200 or 2,000?" In this case, the answer is to team up with an expert in liquid handling.
An intrinsic disadvantage of these manual procedures is poor reproducibility; higher reproducibility can be achieved using automated sample preparation devices.
This concept of "carryover" was very important for the operation of sample preparation devices, as there can be many contaminants in an input sample that could interfere with downstream molecular analyses, and thus represents a critical area of study with the SLIDE device.
XYH carried out most of the sample preparation including device design, e-beam lithography, photolithography and thin film deposition experiments, and conducted electrical measurements of the sub-micron samples.
With the aid of an automated sample preparation system, this device can quantify protein expression, phosphorylation and localization with subcellular resolution at one-minute intervals.
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