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Spectra were collected with a Bruker's ARTAX 200 micro X-ray spectrometer with a Mo anode without any He flush to avoid the tiny sample movement.
Two stripes (stripe 1 and stripe 2) were bombarded with two different plateau fluxes j applying the sample movement scheme described above.
The sample movement during acquisition combines a translation, typically horizontal, along one axis and a rotation about a second axis perpendicular to the first, and is shown to produce theoretically exact CT reconstructions.
The variable focus of the image, combined with sample movement between measurements, means that the ROI signals may suffer from reproducibility problems and that signal crosstalk is a significant problem.
A Staeubli serial six-axis robotic arm offering full six degrees of freedom for sample movement, with a spatial positioning accuracy of the order of tens of microns has been commissioned.
The sample movement is ensured by three types of sample holders for: a) First Wall panels, b) divertor inner vertical target and c) antenna faraday screens as well as other test mock-ups and small-scale samples.
Similar(31)
For deceleration voltages higher than −2.5 keV, focus and astigmatism stability were decreased, and sample movements and distortions became problematic.
Previously, Jinschek and Helveg suggested that charging may lead to resolution degradation by inducing sample movements mediated through a capacitive effect between different parts of the sample.
The usefulness of the approach, including its robustness against axial sample movements, is demonstrated for a multi-layered plastic foil structure.
With the development of direct-detection camera and better algorisms dealing with sample movements and image processing, TRPV1 channel structure in the closed state was determined by cryo-EM at an astonishing resolution of 3.4 Å (Liao et al., 2013).
The tilt of the sample is corrected mechanically prior to the experiment, while drifts and sample movements are corrected by applying algorithms during post-processing.
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