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The intensity curve of the sample, modified for 0.5 h, represents the linear section, the slope of which n1 = 2.4 indicates the formation of the volumetric fractal structure with the dimension of Dv = 2.4.
It should be noted that there are no linear section on the intensity curve of the sample modified for 1 h; that is probably the evidence of the chaotic (non-fractal) distribution of heterogeneities.
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At protocol 1, a high hydrophobicity was observed for sample modified at the first stage with long-chain oligomers (sample 1).
The impedance spectra obtained for PSi modified by potentiostatic mode have been modeled with the same equivalent circuit, but using a CPE for the porous layer while for the sample modified with five CV cycles, a third parallel combination has been added (see inset in Fig. 4f).
Studies have shown that the best quality of copper layer was obtained for a sample modified with 10 laser pulses with fluence of 15 mJ/cm2.
While the water contact angle of the HMDS-modified thin film alumina surface (three successive 4-h cycles) was only (82.9 ± 3)°, the water contact angles obtained for the nanoporous alumina samples modified in HMDS for one and three successive 4-h cycles were (139.2 ± 3)° and (145.3 ± 0.2)°, respectively.
Moreover, the two-sample t-statistic modified for correlation between the two duplicates was used.
CV measurements revealed increased chemical diffusion coefficient values for Li+ ions inside lithium-titanium oxide matrix for samples modified with silver nanoparticles.
However, a dependence on the filler concentration was verified, and the best electrochemical response was obtained for samples modified with 300 ppm of silica nanoparticles.
For samples modified with graphene, no melting peaks were detected that can indicate that graphene hinders crystallization of soft segments.
(b) FTIR-ATR spectra for pSi samples modified with silane (A) and with a layer of pDEAEA spin-coated on the surface (B).
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Justyna Jupowicz-Kozak
CEO of Professional Science Editing for Scientists @ prosciediting.com