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Analyte extraction and sample clean-up is not required.
A quick, easy, cheap, effective, rugged, and safe (QuEChERS) approach is proposed for sample clean-up.
Sample clean-up was achieved by adding acetonitrile for protein precipitation.
Multi-target immunoaffinity columns containing antibodies for all mycotoxins studied herein were used for sample clean-up.
Sample clean-up was achieved by precipitation and solid phase extraction (SPE) with a mixed-mode column.
In general, such matrix effect is directly related to an insufficient sample clean-up of the biofluids.
Chromatographic methods offer a high degree of selectivity but need sample clean-up and relatively heavy instrumentation.
For sample clean-up, 4 ml of the CFP extract was added to 20 ml of concentrated formic acid.
Acceptable baseline was obtained indicating acceptable efficiency of the sample clean-up step in the adopted SPE procedure [31].
The first step is taking aliquots of samples for the analysis, followed by the extraction procedure and sample clean-up, chromatographic analysis and detection.
After sample clean-up, peptide and protein profiles were obtained on an ultrahigh-resolution matrix-assisted laser desorption/ionization Fourier transform ion cyclotron resonance mass spectrometry platform.
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