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So Geim had set one of his new Ph.D. students, Da Jiang, the task of trying to obtain as thin a sample as possible — perhaps a few hundred atomic layers — by polishing a one-inch graphite crystal.
Data were collected at 16,000 keV (λ = 0.77 Å) and 100 K with the Pilatus 6 M detector as close to the sample as possible (179.5 mm).
In order to ensure as clean a sample as possible, a subsequent annealing treatment at 270 °C in a reducing atmosphere and acetone wash was applied leading to near complete removal of residual photoresist, as revealed by our optical images.
Because we are aiming to retain as much of the original IMM sample as possible for the analysis, and because we found little variation in the percentage of the sample in each of these states across the mail months within phase, we did not exclude these cases12.
We chose to apply MALDI-TOF MS on serum processed minimally, aiming to preserve relative protein expression levels as close to the original serum sample as possible.
Due care was exercised to include as many of these pharmacies in the sample as possible.
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Accordingly, it is important to sample as close as possible to the return-period of large-size sediment input events.
The always-hospitable Woodberry's strength is in its small plates and starters; make sure to sample as many as possible -- particularly if there's seafood involved.
All procedures should be optimized as to retain the native spatial distribution and molecular identity of analyte compounds in the sample as far as possible.
It is essential to grind the tissue as finely as possible, maintaining samples as cold as possible during grinding to avoid degradation.
"The idea here is to get as many samples as possible, so the way to do this is to give up a little bit of control," Dr. Fitzgerald said.
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Justyna Jupowicz-Kozak
CEO of Professional Science Editing for Scientists @ prosciediting.com