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The electrocatalytic ability of the modified electrode was tested using hydrazine as a sample analyte, and showed a significant 10-fold improvement in the detection of hydrazine compared to the surface without nanotubes, and comparable stability.
Total antioxidant capacity by phosphomolybdenum method assay is based on the reduction of Mo VI) to Mo(V) by the sample analyte and the subsequent formation of green phosphate/Mo(V) complex at acidic pH [ 3].
This assay is based on the reduction of Mo (VI) to Mo (V) by the sample analyte and the subsequent formation of a green phosphate/Mo (V) complex at acidic pH [ 30].
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Moreover, the thin film method could be used in parallel with the iDEP experiment when the set up allows one to detect dual fluorescence from sample analytes and RhB dye.
By the use of an additional syringe, reagent blank, sample blank, unspecific interferences, and sample analyte concentration was evaluated by simply changing the mode of operation.
In contrast the optimal thionine concentration during continuous regeneration varies with the sample analyte concentration.
For example, brominated diphenyl ether 100 served as the sample analyte for the brominated flames retardants.
Warnken et al. investigated the effects of the DBL (analyte flux decrease) and of lateral diffusion inside the DGT sampler (analyte flux increase) and showed that in standard samplers (A = 3.14 cm, Δ gdl = 0.094 cm) these effects are almost exactly balanced.
Various injection methods have been reported which introduce sample analytes into the GC analytical column.
When the electric potential is applied, the sample analytes of volume 10 μL are loaded onto the sample reservoir.
Method detection limits (MDL) were determined individually for each serum sample and analyte, dependent on volume and blank samples, and were typically in the sub-to-low nanograms per gram lipid range (medians, 0.5 7.8), except DDE (median, 39.6 ng/g lipid) (see Supplemental Material, Table S1).
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