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The manner in which this interacts with the manufacturing route is outlined.
To make this vast but dilute (CH4∼3.9 wt%) energy source available, an economical three-step route is outlined.
The synthetic route is outlined in Scheme 1 and described in detail in the Supporting Information.
The general synthetic route is outlined in Scheme 2. The substituted 6-chlorouracil starting material was made by condensation of the appropriately substituted urea with malonic acid, followed by chlorination.
Similar(56)
Enlightened by Araújo's successful access to furanoside [12], an alternative retrospective route was outlined to obtain the key intermediates 3a and 3b from the readily available 2-deoxy-d-ribose (4a) [13] and d-arabinose (4b) [14], respectively.
These three routes are outlined in Sections 3, 4, and 5 below.
The synthetic routes are outlined in Schemes 1 and 2. The treatment of 1 (1 equiv) with anhydride (1.5 equiv) and DMAP (0.1 equiv) in anhydrous CH2Cl2/pyridine (1/7 = v/v) at room temperature afforded 3-O-acyl derivatives 3a 3c [19, 19, 20, 25] (64 89%).
Several examples of relatively well-characterized routes are outlined in Figure 3.
A route for further investigations is outlined.
The synthetic route to the title compounds is outlined in Scheme 1 [see Additional file 1].
The academic route to a futures qualification is outlined with a list of futures orientated organisations.
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