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In a typical procedure, 0.1 ml aqueous of 0.05 M HAuCl4 was added into 5 ml rGO SDS aqueous dispersion in a 10-ml bottle under rigorous stirring for 1 h.
Next , 10mL 86.2% (w/v) ortho-phosphoric acid was slowly added followed by rigorous stirring for 30 min until the cellulose was completely dissolved.
Both the solutions were mixed and subjected to rigorous stirring for another 20 min.
In a typical process, 93.75 mg of Na2MoO4 · 2H2O and 185 mg of thiourea was dispersed into 30 ml of H2O by rigorous stirring for 5 min.
All solutions were degassed by purging with N2 and with rigorous stirring for a minimum of 2−3 h (1 L of buffer in a plastic flask with minimum head space) before placing in an anaerobic cabinet (Belle Technology; ≤2 ppm O2) overnight at ca. 25 °C.
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After purging with high-purity nitrogen for half an hour, the valves and inlet were closed, and the reactor was immersed into a thermostatic oil bath at 110 and 65 °C for styrene (St) and methyl methacrylate (MMA) polymerization, respectively, under rigorous stirring.
The biphasic medium does not require rigorous stirring.
Following this, 0.6 M thiourea solution was slowly added to the mixture with rigorous stirring.
For a synchronous addition, 10 mL of solutions A and B was simultaneously and stoichiometrically added to a reactor pre-filled with 20 mL of anhydrous ethanol using a syringe pump (model: KDS 270, KD Scientific Inc., Holliston, MA, USA) at a feeding rate of 2 mL·h−1 under rigorous stirring at RT.
Cook, stirring, for two minutes.
Cook, stirring, for 1 minute.
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CEO of Professional Science Editing for Scientists @ prosciediting.com