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In each mixture, 2 mL of pyridine was added, followed by stirring of the resulting solutions for 24 h at room temperature.
The resulting solutions, for the maximum area case, maintain alcohol combustion at low levels showing efficiencies around 63% in each operational level.
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The resulting solution stirred for 8 h at room temperature.
HO2C-buSS-Pyr (280 mg) and diisopropylcarbodiimide (DIC, 436 μL) were then added to the mixture and the resulting solution stirred for 36 h.
The resulting solution was stirred for 1 more hour and left for aging overnight.
The resulting solution was kept for slow evaporation.
The resulting solution was stirred for 4 h at 70 °C.
The resulting solution was stirred for 2 h.
The precipitate was filtered off and the resulting solution was kept for slow evaporation.
The resulting solution was stirred for another 3 h prior to dilution with saturated NaHCO3 (100 mL).
This was followed by incubation of the resulting solution at 50 °C for 20 min.
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