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Linearity, limits of detection and quantitation, repeatability, and trueness of the method were evaluated.
The fortified samples were used for repeatability and trueness (recovery) determination.
Several validation parameters, such as linearity, limits of detection and quantification, repeatability and trueness were also evaluated.
Additionally, the working range, limits of detection and quantification, as well as repeatability and trueness of the method have been evaluated for maize.
Similar(56)
The LoD indicates the level at which detection becomes problematic, while LoQ is the lowest concentration of the analyte that can be determined with an acceptable level of repeatability, precision, and trueness.
The International Standard ISO 5725's statistical methods are used to estimate the repeatability, reproducibility and trueness of a standard measurement method [ 13].
In this paper, the authors introduce additional methods to the mainstream GUM Guide to the expression of uncertainty in measurement for testing laboratories, namely methods based on repeatability or reproductibility and trueness approaches.
The contributions of the repeatability, intermediate precision and trueness were taken into account for the calculation of the expanded uncertainty (U) of the measurements.
Besides the methodological aspects, the obtained analytical results and relevant performance characteristics (e.g. measuring range, limit of detection, repeatability, reproducibility, trueness, and expanded uncertainty of measurement) are determined and discussed.
To use these element-specific methods for quantification relative to the endogenous maize gene hmg it is necessary to perform an in-house validation including relative repeatability and reproducibility standard deviation and trueness.
These values demonstrate sufficient trueness, repeatability, and precision of the method and also the stability of prepared SPAR (SiO2 APAA) for at least 2 weeks storage.
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