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Dissolution and removal of templates were achieved by extensive dialysis against water at temperatures below the LCST of PDEGMA.
The removal of templates was achieved by overoxidation in the presence of 0.05 mol dm−3 NaOH.
A dielectric-barrier discharge (DBD) plasma technique, initiated at ambient conditions, was recently developed for the quick, safe and easy removal of templates from molecular sieves.
Novel mesoporous carbon has been synthesized using rod-like nano-hydroxyapatite (HA) particles as templates, sucrose as carbon precursor by polymerizing, carbonizing and the removal of templates with HCl solution.
In the synthesis of oxide nanotubes, we demonstrate that various oxide nanotubes could be synthesized by the adsorption and hydrolysis of precursors on the surface of carbon nanofiber templates and by the oxidative removal of templates.
Mesoporous materials are generally synthesized via a soft- or hard-template-aided process, which usually, however, suffers from the removal of templates and resultant structural collapse, although hydrothermal synthesis or treatment has been extensively investigated at various stages with the attempt to improve the hydrothermal stability of the as-synthesized mesoporous products.
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The removal of template was performed by refluxing the as-synthesized product in a mixture of methanol and HCl.
Silica-sustained electrospun PVP fibers with uniform mesopores were synthesized via facile oxidative removal of template molecules by H2O2 extraction.
Even after removal of template by solvent extraction and calcination the shape of the nanorods was intact except the generation of pores on the nanorods.
In this work, highly porous Sn C (HPSC) composite was synthesized by a simple carbothermal reduction method followed by a subsequent removal of template.
The template ion leaves cavities of its own shape and size. 1 N HCl solution was used for the removal of template from the polymeric microspheres through sonication for 30 min (three times).
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