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By employing the same direction of Ha, we can derive the following refinement result.
This conclusion is in accordance with the XRD refinement result of NCs, which has been displayed in Figure 2 above.
The refinement result is given by (mathcal {P}_{1} cap mathcal {P}_{2}), a partition with six blocks.
According to the Rietveld refinement result, it is known that Mg2+ takes the tetrahedral 8i sites shared with Li+ in the structure.
Upon Na-doping, Rietveld refinement result reveals that Na takes the tetrahedral sites (8c) shared with Li and Co in the structure.
The Rietveld refinement result clearly exhibited that the cubic spinel phase was successfully formed without any secondary phases, indicating that Li and transition metal cations occupied the 8a and 16d sites of the Fd3m structure, respectively.
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Figure 2 Powder XRD patterns and Rietveld refinement results.
Based on refinement results, the structure was orthorhombic having the lattice parameters shown in Table 1.
Figure 22 shows some refinement results of the five methods for the same transmission maps.
Thus, the refinement results make it possible to propose three coordination modes (Fig. 6).
The refinement results revealed that the lattice constants steadily increased with increasing Co-doping level.
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