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Table 3 shows the cell parameter refinement data of the obtained materials.
Table 2 shows the cell parameter refinement data of the as-synthesized nanomaterials.
Its refinement data are summarized in Table 1 while the bond lengths and bond angles are presented in Table 2.
Table 2 shows the cell parameter refinement data of the obtained materials at different Li/Si molar ratios.
The Rietveld refinement profile is shown in Figure 1c with crystal and refinement data given in Table 1.
Crystal refinement data, selected bond lengths and angles of salts Additional files 4, 5, 6: 5, 9, 10 are tabulated in Tables 1,2,3,4.
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Selected bond lengths and angles are given Table 1 and Crystal and structure-refinement data in Table 2.
Here we go beyond the narrow documentation of final crystallization conditions that produced the refinement-data crystal, to describe the pathway to successful crystallization, data collection and phase determination of this difficult protein with the hope that our experiences will be instructive to others faced with challenging crystallization problems.
Data collection, cell refinement and data reduction were performed with SMART (Bruker, 1998), SAINT Plus (Bruker, 1998) [31] respectively.
Data collection and refinement: Diffraction data for all structures were collected from single crystals at the Diamond Light Source macromolecular crystallography beam lines I02 and I04-1.
The crystallographic data and refinement information are summarized in Table 1.
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