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All frequencies were referenced externally to a 0.1 M AlCl3 solution (δ = 0 ppm).
All chemical shifts are referenced externally to TMS and spectral intensities were normalized by the dry weight of the sample.
Chemical shifts were referenced externally to the methylene (−CH2−) group of adamantane (Sigma-Aldrich) at 38.48 ppm.
All spectra were referenced externally to 80%H3PO44 (0.0 ppm) with downfield shifts represented by positive values.
All indexed files are assigned a globally unique identifier so that they can be unambiguously linked to their metadata and referenced externally even if their location changes.
P{H} NMR spectra were recorded using a JEOL Eclipse 400 MHz spectrometer (operating at 161.8 MHz), referenced externally to 85%H3PO4O4 (aqueous).
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Al and P{H} NMR chemical shifts were referenced (δ=0) externally to 1 M AlCl3 (aq).
13C chemical shifts were externally referenced to the adamantane CH2 signal at 38.48 ppm on the TMS scale.
The 1H MAS NMR spectra were externally referenced using adamantane.
The 13C CPMAS NMR spectra were externally referenced using hexamethylbenzene (HMB).
Chemical shifts were externally referenced to TMS (δ = 0 ppm) using the methyl resonance of hexamethylbenzene (17.5 ppm relative to TMS).
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