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A static extraction time was unnecessary for reducing the extraction time to 1 h.
Detection limits obtained were lower than the olfactory threshold of the studied compounds, being similar or even lower than previously reported with the advantage of reducing the extraction time.
The measurement of extraction curves near optimized conditions (140 °C/055 °C/0 wt.% EtOH and 190 °C/055 °C/0 wt.% EtOH) confirmed the trends of the statistical analysis and revealed that SFE enhances diterpenes concentration by 212 410% at the expenses of reducing the extraction yield between39%and79%79% in comparison to n-hexane extraction.
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The greatest extraction yield was obtained using maceration technique compared to other extraction methods which reduces the extraction time and provides extracts with higher antioxidant activity (Table 1).
Propolis extracts can also be obtained by turbo-extraction, which reduces the extraction time to less than one hour, without using heat.
A set of proposals is now in the making that would reduce the extraction of water available for consumers by up to a third.
Combined with prior literature [34], our ultrasonic extraction method reduced the extraction time obviously.
This method to acquire calibration points can reduce the extraction error.
The results demonstrate that the use of ultrasound and of microwave extractions greatly reduce the extraction time.
Compared to reported extraction methods, the optimal ILEAE method reduced the extraction time significantly and offered higher extraction yield.
Compared with HRE, the modified UAE method reduced the extraction time, the extraction temperature and the solvent consumption.
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