Exact(30)
The amount of recovered solids was insufficient for analysis by XRD.
However, 40 90% of NH4+-N removed was through air stripping instead of being immobilized in the recovered solids.
A small portion of recovered solids (~ 1 mg) were removed from the filter disc and rinsed with deionized water to remove residual aqueous Fe, Mn, and buffer salts.
To reconcile the amount of Fe(II) lost from solution with the production of Mn II) into solution, acid extractions were performed on recovered solids to measure total Fe and Mn species.
Table 1 Sepiolite content of the different synthesis mixtures and yield of recovered solids (wt%) Sepiolite Solid Zeolite Sepiolite Sample In gel Yield Yield a In solid a nMFI 0 4.0 b 4.0 0.0 nMFIsep1 0.37 2.7 c 2.3 13.6 nMFIsep2 1.11 6.2 c 5.2 17.7 nMFIsep3 1.85 7.2 5.4 25.4 nMFIsep4 d 1.86 7.2 5.4 25.5 a assuming sepiolite is fully recovered in the solid.
Composition of recovered solids after 70 °C 5 h [C2C1im][OAc] pretreatment.
Similar(30)
The recovered solid catalyst phase was reused to keep the catalytic activity after several times.
This solids content was used to determine the total recovered solid biomass after the pretreatment.
The recovered solid was lyophilized (Labconco FreeZone(12)) and used for analysis.
The recovered solid was lyophilized (Labconco FreeZone(12), Kansas City, MO, USA) and used for analysis.
After pretreatment, the recovered solid fractions were brought to neutral PH and stored at −20°C for enzymatic hydrolysis.
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