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The MPMS was operated under the reciprocating sample option (RSO) mode.
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After it was subjected to a large-amplitude reciprocating shear, the sample transformed to an oriented hexagonal cylinder (Hex) phase.
To have better control over the thermomechanical history, instead of a reciprocating screw, the samples were prepared by extruding supercooled melt through capillary die.
This approach is demonstrated by a preliminary study of the coefficient of friction (CoF) in sub-mm length reciprocating sliding motion for samples of polytetrafluoroethylene (PTFE) and an R11 acrylic formulation made by micro-stereo-lithography, with an SiO2-coated silicon wafer used as a control sample.
Reciprocating wear tests comparing a PVD nitrided sample, an untreated sample and different laser nitrided samples indicated that the laser nitrided sample with the lowest surface roughness exhibited the least amount of wear and had the lowest friction coefficient.
To accomplish this, a reciprocating friction tester and test samples were designed and fabricated.
Cumulative formation can take full advantage of available sampling information and avoid reciprocating oscillation in the iterative process.
In order to investigate the wear properties, the samples were subjected to reciprocating wear tests against AISI 4140 pin under dry sliding conditions.
Spectra at room temperature were recorded in a 90° scattering geometry on samples mounted on a reciprocating translation stage.
The tribological properties of the coated and uncoated samples are investigated using a reciprocating sliding wear tester in NaCl solution.
Wear tests were carried out using a ball on flat reciprocating micro-tribometer between a diamond probe and the samples under dry sliding conditions.
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