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Raman and photoelectron spectroscopies show that the reaction is complete within 90 s of immersion.
After the reaction is complete, nitrogen with a flow rate of 3 l/min was introduced to furnace to cool down the system and to prevent the air entering the system.
On the other hand, the pulses of 1 min allow to monitor when the reaction is complete by TLC, especially, in cases of the compound 4n which reaction time was 45 min.
The solubility constant for tobermorite was determined from the water composition for t = 4.5 8 d samples, where the XRD data suggests that reaction is complete and the solution is fully saturated with respect to tobermorite (Figure 12).
Results show that there is an optimum initial redox potential range between 1 340 and 1 819 mV, at which the extent of graphite layer oxidation is moderate and the intercalation reaction is complete.
Without an iron catalyst, the reaction is complete after several hours (~7), when no further weight increase due to nitrogen absorption (per gram of silicon) is detected.
Similar(32)
The reaction is completed in 30 minutes at reflux.
Once the reaction is completed, the solution is cooled to room temperature.
After the reaction is completed two clear liquid phases occurred that can be easily separated.
Once the reaction is completed, the flask is cooled to 0°C before addition of cold satd.
After the reaction is completed the reboiler contents are cooled, weighed and analyzed.
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