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Under optimized conditions, Hantzsch reaction conducted well, resulting in a yield of 98.7% and excellent selectivity.
A novel strategy for a heterogeneous benzylation reaction conducted in a capillary microreactor was proposed.
When the reaction conducted in a one-pot consecutive way, the yield of glycidol was 20%.
But the liquid-phase reaction conducted in the batch-type reactor exhibited the same olefin addition effect.
This phenomenon was not observed in the gas-phase reaction and liquid-phase reaction conducted in the trickle bed.
A process involving an exothermic reaction conducted in a semi-batch reactor is used to demonstrate the advantages of the proposed procedure.
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Graphical abstract The biocatalytic reactions conducted with the recombinant AcCR.
Catalytic reactions conducted at 340 °C, 3.5 MPa, 250 Nm3/m3 (H2/Oil ratio) and 7.2 h−1 using feed 2 as feedstock.
Table 4 gives the details of the results for reactions conducted with different substrates.
The organic solution was added into aqueous solutions slowly, and the mixture was kept overnight until the reactions conducted completely.
The shape of the curve presented in Fig. 6a is common for most of the dissolution reactions conducted for this study in both reaction media.
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