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The ESEM images of geopolymers containing 4 10 wt% of HAP showed some non-reacted or partially reacted particles that do not well connect to the matrix.
High-resolution X-ray photoelectron spectroscopy (HR-XPS) analysis of the reacted particles indicated that Hg II) was sequestrated via chemical reduction to elemental mercury.
To investigate the reaction process inside the pellet, microscopic analyses and REM/EDX element scans of reacted particles after different reaction times were performed.
The ability of the particles to withstand impacts was also investigated by examining the degree of fragmentation of 1 g of reacted particles of known size on projecting them at a target at various velocities.
If reacted particles run out the center of the capsule, its energy will be wasted.
They reflect the light protons, D, and T, repel high-energy reacted particles (4He, p) back to fuel, and significantly (in hundreds time) increase the conformation time.
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With mixtures of water and HCl, however, the ratio of CaO to CaCl2 in the reacted particle varied with the concentration of water.
At moisture levels typically found in combustion products, a fully reacted particle contained about 66 wt% CaO and 34 wt% CaCl2.
Figure 5 (A) Partially reacted particle and (B) X-ray map. Figure 5A shows a partially decomposed particle made of a gel halo, a reaction front and an unreacting core.
The light emission from the reacting particles was monitored.
The model allows for intraparticle temperature gradients and shrinkage of the reacting particles.
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