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However, annealing and quenching of samples followed by transmission electron microscopy and Raman spectroscopy revealed an order disorder phase transition at ∼1200 °C.
In the case of CoA esters, sampling and quenching of samples was performed as described [31].
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Shaking and quenching of the samples were done immediately, and the centrifuge tubes with the sample were kept in an ice bath immediately.
Post annealing and quenching of the samples were used to investigate the order disorder phase transformation temperature of Cu5Zn8 in the nanosized form.
Also, we showed that rapid quenching of sorption samples for data collection at low temperature does not appear to introduce any new features into EXAFS spectra when compared with room temperature spectra.
Use of a calibrated digital multichannel pipette further reduces assay variability by allowing rapid treatment and quenching of many samples nearly simultaneously.
Metabolic quenching of the samples was by the injection of RNA later (Ambion, Life Technologies, Darmstadt, Germany).
In the second variation, quenching of incubated samples was with 100 μL of a suspension of DEAE cellulose (Whatmann DE52 preswollen, 16 mg of resin per 100 μL of water) followed by 400 μL of ethyl acetate.
Quenching of the samples was achieved by quickly adding 20 mL of cell culture to 30 mL cold methanol (83.3 % methanol in water) in pre-cooled 50 ml conical tubes.
Figure 3a,b shows Ga droplets on a GaAs surface prepared with immediate quenching of the sample after droplet deposition (ta= 0).
While the as-synthesized samples show a positive thermal quenching of luminescence, the samples annealed at 200 °C show novel negative thermal quenching of emission with increasing measurement temperature.
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