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The procedure, based on direct SPME at 50 °C, using a polydimethylsiloxane fiber, showed good linearity (r > 0.997 over a concentration range 2 200 μg L−1) and repeatability (relative standard deviation (RSD) < 4.23%) for all compounds, with limits of detection ranging from 0.05 to 0.28 μg L−1, and limits of quantification ranging from 0.14 to 0.84 μg L−1.
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Limit of quantification ranged from 0.02 to 0.08 mg kg−1.
The limit of quantification ranged from 0.2 μg/kg to 5 μg/kg.
The limit of quantification ranged from 0.1 to 10 ng mL−1, and the recoveries were 34.6 50.3%.
The limits of quantification ranged from 1.0 μg/kg to 12.5 μg/kg for the dinotefuran and UF enantiomers.
The limit of quantification ranged from 0.063 pg m−3 to 0.210 pg m−3 when air volumes of 723 m3 were collected.
Under optimized conditions, the limits of detection and quantification ranged from 0.04 to 0.09 and 0.15 0.29 μg L− 1, respectively.
Limits of quantification ranged from 0.06 to 0.16 ng mL−1 for PCBs and from 0.12 to 0.36 ng mL−1 for organochlorine pesticides.
The limits of detection and limits of quantification ranged from 0.06 mg L−1 to 0.14 mg L−1 and from 0.20 mg L−1 to 0.48 mg L−1, respectively.
The limits of quantification ranged from 0.4 to 0.7 ng mL−1, while inter- and intra-day variability was under 11.1% in all cases.
Utilizing the World Health Organization International Standard for Hepatitis D Virus RNA, the lower limit of detection was 575 IU/mL, and the linearity of quantification ranged from 575,000 IU/mL to 575 IU/mL.
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