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The competitive molecule successfully served as calibrator for quantification, matrix normalisation, and inhibition control.
The current amounts at the given concentration (1 mM) were identified to produce the quantification matrix at each oxidation potential point that was measured without CD immobilization.
To accomplish this task, we developed a risk quantification matrix and a risk register form to identify potential risks in the operating room, and then implemented operating room policies designed to reduce or eliminate those risks.
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For quantification, matrix-matched pellets were prepared with cellulose powder and softwood pulp, doped with multi-element standards.
Validated limits of quantification in matrix were between 0.02 and 1 µg L−1, depending on the compound.
By a novel modification of the correlation constraint in MCR-ALS, quantification despite matrix effects is made possible.
The lower limit of quantification (LLO Q, matrix effect, extraction recovery, stability and dilution integrity were also validated and satisfied with the criteria of validation.
The lower limit of quantification (LLO Q, matrix effect, extraction recovery, stability, dilution test and carryover test were also validated and satisfied with the criteria of validation.
Analytical performance was determined in terms of linearity, intra- and inter-assay precision, detection and quantification limits, matrix effect, accuracy, and drug stability in real samples.
These three endpoints were: quantification of matrix incorporated calcium by (1) morphometric analysis and (2) measurement of calcium levels as well as (3) activity of alkaline phosphatase, an enzyme involved in matrix calcification.
(B) The quantification of matrix degrading activity was performed as described in section " Methods ".
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