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A validation study included linearity, precision, detection and quantification limits.
The detection and quantification limits were 12 and 40 ng/g, respectively, for all analytes, except carbaryl (detection and quantification limits 3 and 10 ng/ng, respectively).
Detection and quantification limits of the method were determined as described previously.
The quantification limits determined for all other compounds were between 3.0 and 0.7 µg m−3.
Quantification limits were calculated to a signal-to-noise (S/N) ratio of 10.
For these data quantification limits (LOQ) were reported, which are 3.3 times the detection limit.
The lowest quantification limits were from 0.002 to 0.6 μg/L for 1.0 mL of saliva.
Statistical analysis allowed establishing parameters like linearity, detection and quantification limits, recovery, precision and trueness.
The residential SCTL is also near the practical quantification limits using analytical procedures.
The detection and quantification limits were 0.03 and 0.1 μg L−1, respectively.
The quantification limits for the two fibers varied between 1.0 and 10.0 ng L−1.
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