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Platform evaluation and analysis method selection using quality control samples.
developed and prepared breast xenografts used as quality control samples.
K.F.S., L.J.Z., R.J.C.S. and D.C.L. directed and performed proteomic analysis of colon tumour and quality control samples.
The supernatants were subjected to global metabolomic analysis, and pooled samples were used as quality control samples.
During assay development a significant loss of A was apparent from frozen urine quality control samples.
In addition, 2 quality control samples (500 pmol/g liver analyte level) were measured together with the study samples to ensure proper analysis.
Calibrants and quality control samples were prepared using blank hair.
Variability of the quality control samples was assessed from the validation procedure.
The quality control samples were prepared from an independent weighing of the reference standard.
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The interassay precision for the low- and high-quality control samples was 2.2 and 1.4%, respectively.
Duplicate quality-control samples (2% of the total) showed 100% agreement for all 25 assays.
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