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The measurement was carried out at 79.4 MHz and single-contact cross-polarization pulse program was used.
As standard pulse program, the water suppression Watergate W5 pulse sequence with gradients using double echo was taken [5].
IR results were useful to set a potential pulse program which allowed to adsorb dissociatively the organic compound.
After this modified pulse sequence, the standard pulse program with 16 scan was used to record the spectra for the analysis of the hydrolysis.
The writing processing, i.e., voltage level programming, is realized by incremental step pulse program with an incremental program step voltage Δ Vpp [4].
After each pulse program or erase operation, the test circuit is switched by the matrix to 4200 to read the resistance (Figure 3a,d).
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By using an incremental step pulse programming algorithm, its read window can remain stable after 1 million cycles.
NMR spectra were recorded on a Bruker AM-400 spectrometer (Bruker, Karlsruhe, Germany) using standard Bruker pulse programs.
b One million cycles endurance test result of the STI-RRAM using Incremental Step Pulse Programming algorithm.
The incremental step pulse programming (ISPP), which is the most widely used programming scheme, was proposed to maintain a tight cell threshold voltage distribution for high reliability[7, 8].
In flash memories, distances between 2 M states can be controlled by adjusting verify levels during incremental step pulse programming (ISPP).
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